So you desire the MHRB layer to generally be BLACK. That’s how you are aware of you attained the correct pH. If it isn’t, you are able to consider incorporating a lot more NaOH however, if it begins to NOT dissolve, you need to incorporate a lot more water (distilled or filtered). You then’re probably planning to must increase additional Naph
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There is nothing Mistaken when your Answer turns thick. It will initial begin to convert gray and it will get really thick like molasas. Then it will start tirning black and can go back to a watery liquid. Its crucial that you retain every thing warm your complete time right until you visit freezer. Use double boiler system to keep the alternatives